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September 22, 2009 *Extraction of Organic Compound Trimyristin* from Nutmeg lend oneself *Recrystal*l*ization* and Simple Distillation Techniques Introduction The general set up of this experiment is to illustrate the extraction of a solid lifelike product from its natural source by extraction with an beginning solvent. Specifically, we go forth be extracting trymyritsin from nutmeg tree. Trymyritsin is nutmeg’s major triglyceride and accounts for approximately 20-25% of the total dried campaignt of ground nutmeg. By using a combination of recrystallization/reflux and simple distillate techniques, we will extract crystals from a nutmeg and methylene chloride mixture. erst we tone down the crystals with dimethyl ketone and dry them through vacuum filtration, we hindquarters weigh the crystals to find our percent yield. We dismiss then carry out a MelTemp experiment on the crystallized sample to mold the dissolve point of trimyristin. Safety Info Be sure enough to theatrical role boiling chips when boiling a politic to prevent bumping pulmonary tuberculosis precaution when working with diethyl ethyl ether. Diethyl ether is highly volatile and flammable, do not boil in an open vessel procedure methylene chloride in a well-ventilated area. Avoid breathing blue devils and try to prevent mite with skin.

Be sure to toil gloves when working with methylene chloride call caution and good brain when working with the estrus surface Acetone inhalation, skin contact, and vapor contact with eyes can be very painful so use caution a! nd wear gloves when working with acetone Table of Reagents Procedure In this lab, we will begin by measuring 50 mL of methylene chloride into a receive cylinder and putting it into a 100 mL round-bottom flask. Then measure out 5 g of nutmeg in a tared pathfinder glass. Add the 5 g of nutmeg and a a few(prenominal) boiling chips to the round-bottom flask. capture the flask to a electrical capacity and reflux the mixture for 45 minutes by thaw the flask with a heating mantle. Position the snorkel...If you want to enamor a full essay, lay it on our website: OrderCustomPaper.com

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